Make Anhydrous Ferrous Chloride

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Videos referenced in this video:

Make chlorotoluene: https://www.youtube.com/watch?v=khfYvY_Gczk

Make ferric chloride (hydrated): https://www.youtube.com/watch?v=43Xsh9J7S-g
In this video we make ferrous chloride.

First we react 57g of iron metal with 200mL of 30% hydrochloric acid and 300mL of methanol. Once hydrogen evolution ceases the mixture is filtered. One or two large iron nails are placed in the flask and an air-tight simple distillation is assembled. The exhaust port on the distillation adapter is connected to a vacuum system and the distillation is performed under reduced pressure. Once the ferrous chloride is dried, the flask is stoppered and stored until needed.
This video was generously sponsored by:
Robert Boll
Kevin S
Only HR
Scott Malcheski
advisable
Michael Zappe
Emil Mikulic
Dino Capiaghi
Benjamin Nied
Wesley Gardner
LVE
Meshal Al-Enazi
Lord Martin Hill
Matthew Brunette
Collin Wright
Simon Bitdiddle
Cullen Purkis
Samuel Pelzer
Carl Potter
Max Loutzenheiser
Jack kelly
Phillip Hutchings

Видео Make Anhydrous Ferrous Chloride канала NurdRage