Making Trinitromethane/Nitroform (Part 1)

In this video I make what I believe is trinitromethane in possibly the worst yields known to man. I hope to improve this result in future. The extraction method seems kind of bad. The usual method involves distillation but I was worried about that causing an explosion. To simulate this in a more safe manner, I instead extract with DCM and then throw my flask onto the concrete.

Production: http://www.google.com.au/patents/US4122124
Extraction: http://patents.justia.com/patent/4147731

Видео Making Trinitromethane/Nitroform (Part 1) канала Extractions&Ire