Cubane Episode 3 - Vacuum Distillation for the Ketal?

Following on from the Dean stark nonsense last video, we clean up our product and attempt to work out how to do a vacuum distillation. What could possibly go wrong??

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Paper we are following: https://www.researchgate.net/publication/244572672_Dimethyl_Cubane-14-dicarboxylate_A_Practical_Laboratory_Scale_Synthesis

Music is as usual from the Aphex Twin soundcloud dump, track names is

Polygon Window - clissold 101[dat28 otari] 48k

Видео Cubane Episode 3 - Vacuum Distillation for the Ketal? канала Extractions&Ire